Download Instructor's Solutions Manual to Fundamentals of Analytical by Douglas A. Skoog, Donald M. West, F. James Holler, Stanley PDF

By Douglas A. Skoog, Donald M. West, F. James Holler, Stanley R. Crouch

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The within day variance, SSE, reflects the method variance, SSM. The day-to-day variance, SSF, reflects the sum of the method variance, SSM, and the sampling variance, SSS; SSF = SSM + SSS. 58. 19. 08333). 4 Fundamentals of Analytical Chemistry: 9th ed. 8-12. 1 × 104 / 454 = 15 lb; Since the seller took only a 5 lb sample and 15 lbs was needed, this is insufficient. 8-13. 36 for 8 samples = N The iterations converge at between 7 and 8 samples, so 8 should be taken for safety. 5 Fundamentals of Analytical Chemistry: 9th ed.

7-31. 970. 10 cannot be rejected with 95% confidence. 829. 10 can be rejected with 95% confidence. 7-32. 710. 60 ppm cannot be rejected with 95% confidence. 16 Fundamentals of Analytical Chemistry, 9th ed. Chapter 8 Chapter 8 8-1. The sample size is in the micro range and the analyte level is in the trace range. Hence, the analysis is a micro analysis of a trace constituent. 8-2. The objective of the sampling step is to produce a homogeneous laboratory sample of a few hundred grams or less having a composition that is identical to the average composition of the bulk of the material being sampled.

7-32. 710. 60 ppm cannot be rejected with 95% confidence. 16 Fundamentals of Analytical Chemistry, 9th ed. Chapter 8 Chapter 8 8-1. The sample size is in the micro range and the analyte level is in the trace range. Hence, the analysis is a micro analysis of a trace constituent. 8-2. The objective of the sampling step is to produce a homogeneous laboratory sample of a few hundred grams or less having a composition that is identical to the average composition of the bulk of the material being sampled.

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